Last updated April 24, 2025

ASTM E595 Standard Test Method for Total Mass Loss and Collected Volatile Condensable Materials from Outgassing in a Vacuum Environment

The ASTM E595 test method is a very important standard for testing the outgassing properties of materials in vacuum conditions. It measures the total mass loss (TML) and the volatile condensable materials collected (CVCM), to ensure that materials are compliant with the stringent specifications of aerospace, electronics, and other high-reliability industries. The test is essential to eliminate contamination of delicate environments like spacecraft and semiconductor fabrication.

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    ASTM E595 Introduction

    Materials to be used in vacuum environments, like in space or high-precision manufacturing, need to have low outgassing. Outgassing causes contamination, which impacts performance and life. ASTM E595 offers a standardized test for assessing these materials by quantifying TML and CVCM. TML is the weight percent of weight lost by a material resulting from outgassing, and CVCM is the measurement of the volatile materials that condense on a collector plate. The standard is especially important in space exploration, where materials for use in satellites and spacecraft must not degrade or contaminate optical and electronics systems.

    ASTM E595 Test Method

    Sample PreparationThe material sample is cut to a specified size and weighed before testing.
    Vacuum ExposureThe sample is placed in a vacuum chamber at 125°C for 24 hours while outgassed materials are collected.
    Data CollectionAfter cooling, the sample and collected condensable materials are reweighed to determine TML and CVCM.

    ASTM E595 Equipment and Sample Preparation

    Vacuum ChamberMaintains a pressure below 10^-5 torr to simulate space conditions.
    Quartz Crystal MicrobalanceMeasures mass changes with high precision to detect outgassing.
    Weighing BalanceDetermines initial and final weights to calculate TML and CVCM.

    ASTM E595 Results and Interpretation

    E595 test results offer essential information about material applicability to vacuum conditions. TML should be in general lower than 1.0%, whereas CVCM should not exceed 0.1%. Any materials above these values might have to undergo treatments like surface coating or alternative material substitution. Results enable engineers to apply only low-outgassing materials in the case of crucial environments, mitigating contamination risk and system failure. The information is of special importance for industries that engage in spacecraft engineering, optics, and precision electronics, where contamination control is crucial.

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    Related Articles

    ASTM E595-related research and developments involve alternative low-outgassing materials studies, polymer formulation advancements, and vacuum testing methodology improvements. Additional reading may involve articles on NASA’s Material Guidelines, ISO vacuum material standards, and comparative studies of outgassing characteristics of different polymers and adhesives.

    Applications in Industry

    E595 is a common test in multiple industries, such as aerospace, semiconductor fabrication, and precision optics. It prevents spacecraft, satellite, and space station materials from contaminating sensors, lenses, or thermal control surfaces. It is used by semiconductor companies to provide clean environments for wafer fabrication processes. Optics companies utilize it to ensure coatings and adhesives do not degrade over time due to outgassing. This method of testing is vitally important for material selection and qualification in those industries with critical vacuum performance.

    Process for testing
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    • STEP 02

      You share your sample(s)

    • STEP 03

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